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Updated: Sep 18, 2025

Profiling Volatile Compounds in Blackcurrant Fruit using Headspace Solid-Phase Microextraction Coupled to Gas Chromatography-Mass Spectrometry
Published on: June 9, 2021
Does Embracing New Approaches in Homemade Fruit Spirit Production Lessen Consumer Health Risks?
Katarina Bijelić1,2, Ljilja Torović1,2, Boris Milijašević3
1Department of Pharmacy, Faculty of Medicine, University of Novi Sad, Hajduk Veljkova 3, 21000 Novi Sad, Serbia.
Using a dephlegmator in small-scale fruit spirit production reduces methanol risks and improves consistency. While helpful, it
Area of Science:
- Food Science
- Distillation Technology
- Analytical Chemistry
Background:
- Traditional fruit spirits are made in Eastern and Central Europe.
- Homemade spirits have inconsistent quality and safety due to variable conditions.
- Harmful volatile compounds like methanol and acetaldehyde pose risks.
Purpose of the Study:
- To assess if a dephlegmator reduces health risks from volatile compounds in small-scale spirit production.
- To determine if dephlegmator use improves product consistency.
Main Methods:
- Investigated 35 fruit spirit samples.
- Utilized Head-Space Solid-Phase Microextraction Gas Chromatography-Flame Ionization Detection (HSS-GC-FID).
- Conducted a risk assessment using the margin of exposure approach.
Main Results:
- Dephlegmator use lowered median methanol concentrations (1878 vs. 3723 mg/L) and narrowed the concentration range.
- No significant reduction in median levels for other analytes, but ranges narrowed.
- Dephlegmator usage increased the proportion of methanol-safe samples.
- Acetaldehyde risk remained equivalent or increased; higher alcohols and ethyl acetate posed no risk.
Conclusions:
- Dephlegmator use is a beneficial but insufficient intervention for safer, consistent small-scale fruit spirit production.
- Further optimization of distillation cuts is needed to manage acetaldehyde risks.
- Ensuring product safety and quality requires a multi-faceted approach beyond dephlegmator use.
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