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Towards high-performance solid-state lithium batteries via antimony doping solid electrolytes.

Jingrui Kang1, Meng Niu1, Zexuan Qi1

  • 1College of Electronic Information Engineering, Key Laboratory of Brain-like Neuromorphic Devices and Systems Hebei Province, Hebei University, Baoding 071002, PR China.

Journal of Colloid and Interface Science
|July 22, 2025
PubMed
Summary
This summary is machine-generated.

Antimony doping enhances lithium aluminum titanium phosphate (LATP) solid electrolytes for lithium-metal batteries. Optimized LATP shows improved density and ionic conductivity, enabling stable battery cycling and high capacity retention.

Keywords:
Electrochemical performanceIonic conductivityLATPSb(5+) dopingSolid-state batteries

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Solid-State Batteries

Background:

  • Lithium aluminum titanium phosphate (LATP) is a promising solid electrolyte for lithium-metal batteries (LMBs) due to its cost-effectiveness and air stability.
  • Practical application of LATP is hindered by low density and high ionic resistance.
  • Developing advanced solid electrolytes is crucial for next-generation energy storage.

Purpose of the Study:

  • To improve the density and ionic conductivity of LATP solid electrolytes.
  • To investigate the effect of antimony (Sb5+) doping on LATP properties.
  • To evaluate the electrochemical performance of Sb5+-doped LATP in LMBs.

Main Methods:

  • Synthesis of a series of antimony-doped LATP materials (Li1.3Al0.3Ti1.7SbxP3-xO12, LATPSx) with varying Sb concentrations (x = 0–0.05).
  • Characterization of relative density and ionic conductivity of the synthesized electrolytes.
  • Fabrication and electrochemical testing of Li|LATPS0.04|Li symmetric cells and Li|LATPS0.04|LiFePO4 full cells.

Main Results:

  • Optimized LATPS0.04 exhibited a higher relative density (98.83%) and ionic conductivity (6.23 × 10^-4 S·cm^-1) compared to bare LATP (96.23%, 1.22 × 10^-4 S·cm^-1).
  • The Li|LATPS0.04|Li symmetric cell demonstrated stable cycling for over 1700 hours at 0.2 mA·cm^-2.
  • The Li|LATPS0.04|LiFePO4 full cell achieved an initial discharge capacity of 153.78 mAh·g^-1 at 0.1C and retained 95.50% capacity after 300 cycles at 1C.

Conclusions:

  • Sb5+ doping significantly enhances the density and ionic conductivity of LATP solid electrolytes.
  • The improved LATPS0.04 electrolyte enables stable cycling and high capacity retention in LMBs.
  • Sb5+ doping is a viable strategy for developing high-performance solid electrolytes for advanced lithium-metal batteries.