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Quantitative Hardness Measurement by Instrumented AFM-indentation
Published on: November 22, 2016
Characterization of Hard Coatings Using Acoustic Emission
Ivana Sára Škrobáková1, Peter Gogola1, Marián Palcut1
1Institute of Materials Science, Faculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Ulica Jána Bottu 25, 917 24 Trnava, Slovakia.
Abstract:
Acoustic emission (AE) testing is a non-destructive method used in various applications. In our work we demonstrate its capabilities and potential in studying the functional properties of physical vapor deposited (PVD) coatings. The goal was to classify the coating damage during indentation testing more objectively by quantifying specific imprint features. The AE response was systematically recorded in nine sample conditions and 27 individual imprints, allowing us to identify correlations between the numerical values derived from the SEM observations and the characteristics of the AE signal. An increase in the delaminated coating area was found to correspond to an exponential increase in the AE signal energy. These findings suggest that AE analysis could reduce the reliance on SEM-based evaluation and help accelerate systematic research in the field of PVD coatings. The advantages of AE testing are discussed and conclusions for practical applications are provided.
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