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Beyond serendipity: uncovering novel ratiometric urea·24DHBA cocrystals through mechanochemistry and MicroED
Ankur Bonia1, Diptajyoti Gogoi1, Nabadeep Kalita1
1Department of Chemistry, Gauhati University, Guwahati 781014, India. ranjit.thakuria@gauhati.ac.in.
Abstract:
Mechanochemical synthesis of urea cocrystals with 2,4-dihydroxybenzoic acid (24DHBA) reveals two new stoichiometric forms: (urea)2·(24DHBA) and (urea)2·(24DHBA)2, not accessible via solution methods. The known (urea)0.5·(24DHBA) form remains the most stable. These findings provide critical insights into stoichiometric tuning of agro-cocrystals and pave the way for their practical application in sustainable agriculture.
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