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Approach and setup to measure high thermal conductivity in multigraphene materials.
V Yu Gubin1, D V Vakhrushin1, N S Morozov1
1Department of Chemistry, Lomonosov Moscow State University, Moscow 119991, Russia.
The Review of Scientific Instruments
|March 2, 2026
Summary
A new setup accurately measures high thermal conductivity materials (λ > 300 W×m⁻¹×K⁻¹). This method, validated on graphite and multigraphene, improves upon existing techniques by accounting for heat loss, ensuring reliable material characterization.
Area of Science:
- Materials Science
- Thermal Engineering
- Nanomaterials
Background:
- Accurate measurement of high thermal conductivity (λ > 300 W×m⁻¹×K⁻¹) is crucial for advanced materials.
- Existing methods like laser flash assay and HotDisc have limitations in certain applications.
- Developing novel measurement techniques is essential for characterizing novel materials like multigraphene.
Purpose of the Study:
- To develop and validate a novel setup for measuring high thermal conductivity materials.
- To assess the accuracy of the developed method by comparing it with established materials and techniques.
- To improve the reliability of thermal conductivity measurements, especially for materials like multigraphene.
Main Methods:
- Development of a measurement approach based on establishing temperature gradients and thermal flows.
- Integration of hardware and software for data acquisition and processing.
- Computer modeling of heat distribution and loss to enhance measurement accuracy.
- Experimental validation using materials such as copper, aluminum, isotropic graphite, and multigraphene.
Main Results:
- The developed setup successfully measured thermal conductivity for various materials, including multigraphene (λ ∼ 500 W×m⁻¹×K⁻¹).
- Computer modeling revealed a 2% overestimation in raw data for multigraphene due to heat losses, which was corrected.
- The device demonstrated reliable measurements, complementing existing instrumental capabilities.
Conclusions:
- The designed device provides accurate and reliable measurements for high thermal conductivity materials.
- The method effectively accounts for heat losses, improving measurement precision.
- This approach offers a valuable alternative or complement to laser flash assay and HotDisc for thermal conductivity characterization.

