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Preliminary Investigation on Mandarin Peel Extraction and Development of Functionalized Chitosan-Guar Gum Edible
Miriam Arianna Boninsegna1, Slaven Jurić2, Amalia Piscopo1
1Department of AGRARIA, University Mediterranea of Reggio Calabria, Via dell'Università 25, 89124 Reggio Calabria, Italy.
Foods (Basel, Switzerland)
|March 14, 2026
Summary
Mandarin peel bioactives were extracted and incorporated into edible films. These functionalized films show excellent properties, supporting sustainable packaging solutions.
Area of Science:
- Food Science and Technology
- Biomaterials Science
- Sustainable Packaging
Background:
- Citrus processing generates substantial by-products rich in bioactive compounds.
- These by-products are often underutilized, representing a loss of valuable resources.
- Mandarin peel (Citrus reticulata) is a promising source of functional compounds.
Purpose of the Study:
- To optimize the extraction of bioactive compounds from mandarin peel.
- To develop functionalized edible films using guar gum, chitosan, and mandarin peel extract.
- To evaluate the functional properties of the developed edible films.
Main Methods:
- Response surface methodology was employed for optimizing both bioactive extraction and edible film formulation.
- Extraction parameters optimized included time, solvent composition, and solvent/solid ratio.
- Film formulation variables included guar gum/chitosan ratio, glycerol content, and extract concentration.
Main Results:
- Optimized extraction yielded significant amounts of total polyphenols (329.59 mg GAE/g), flavonoids (42.6 mg QE/g), and carotenoids (1.53 mg/g) with high antioxidant activity.
- The composite edible films exhibited excellent functional properties: swelling index (65.83%), water absorption (65.48%), weight loss (41.91%), and desirable visual appearance (L* 89.30).
- Predictive models demonstrated high statistical significance and good agreement between predicted and experimental values.
Conclusions:
- Mandarin peel is a valuable source for extracting bioactive compounds with significant antioxidant properties.
- Guar gum/chitosan composite films incorporating mandarin peel bioactives possess excellent functional characteristics.
- This research advances biopolymer-based approaches for sustainable packaging by utilizing food industry by-products.

