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Updated: Aug 5, 2026

Quantitative Hardness Measurement by Instrumented AFM-indentation
Published on: November 22, 2016
Deep Indentation of Soft Thin Films Beyond the 10% Rule
1Peking University, School of Mechanics and Engineering Science, State Key Laboratory for Turbulence and Complex Systems, Beijing 100871, China.
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Indentation is one of the simplest ways to feel the stiffness of matter. Interpreting indentation, however, requires care, especially for thin films-such as biological cells or soft coatings supported by rigid substrates-because the substrate effect can make a film appear orders of magnitude stiffer than it actually is. To minimize this artifact, the empirical "10% rule of thumb," which limits indentation depth to one-tenth of the film thickness, has often been adopted, though it becomes unreliable and impractical for ultrathin films. Here, we explore the traditionally forbidden regime: deep indentation, where the indentation depth is comparable to the film thickness. We develop an asymptotic theory that incorporates nonlinear geometry and elasticity, elucidating a simple indentation force-depth relation in this deep regime. We further show that the pull-off force in such indentation tests is remarkably independent of both the material law and geometric nonlinearity. The results provide a unified framework for interpreting thin-film mechanics under deep indentation, a regime that is generally much more accessible in experiments on very thin films.

