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[Determination of fibrinogen concentration in blood plasma by the sulfite precipitation method]

L A Tsariuk, V N Rybachuk, L I Shevchenko

    Voprosy Meditsinskoi Khimii
    |January 1, 1979
    PubMed

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    Precipitation Titration: Overview01:26

    Precipitation Titration: Overview

    Precipitation titration involves the reaction of a titrant and an analyte to generate an insoluble precipitate. While precipitation titration uses various precipitating agents, silver nitrate is the most common precipitating reagent; titrations involving Ag+ are called argentometric titrations. Usually, the endpoint in a precipitation titration can be detected by visual indicators.
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    Precipitation Titration Curve: Analysis01:21

    Precipitation Titration Curve: Analysis

    The precipitation titration curve demonstrates the change in concentration of one reactant with the volume of titrant added. During the titration of chloride ions with silver nitrate, the precipitation titration curve is divided into three regions: before, at, and after the equivalence point. Before the equivalence point, low redissolution of the sparingly soluble silver chloride precipitate gives a low silver ion concentration. However, in the second region, representing the equivalence point,...
    Precipitation Titration: Endpoint Detection Methods01:19

    Precipitation Titration: Endpoint Detection Methods

    In argentometric precipitation titrations, endpoints can be detected visually by the Mohr, Volhard, and Fajans methods. In the Mohr method, adding a soluble chromate indicator gives an initial yellow color to the analyte solution. As the titrant is added, the first excess of silver ions forms a red silver chromate precipitate, marking the endpoint. The solution pH should be maintained at about 8 by adding solid CaCO3.
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    Precipitation and Co-precipitation01:17

    Precipitation and Co-precipitation

    Precipitation and coprecipitation methods can be used to separate a mixture of ions in a solution. In qualitative inorganic analysis, ions that form sparingly soluble precipitates with the same reagent are separated based on the differences in solubility products. For example, consider the separation of Cu(II) and Fe(II) ions by precipitation as insoluble sulfides. First, copper(II) sulfide is precipitated by the addition of acidic H2S, where the dissociation of H2S is suppressed. Adding H2S...