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Synthesis and structural characterization of a Re(V) complex with a 2N1S donor and the radiochemical behavior of its
P Chattopadhyay1, Y H Chiu, J M Lo
1Department of Nuclear Science, National Tsing Hua University, Hsinchu, Taiwan, ROC.
Abstract:
A rhenium(V) complex with 2-(2-pyridylmethylthio)-aniline has been synthesized and characterized by UV-VIS absorption, IR, MS and X-ray crystallography. The complex contains a ReO3+ moiety and the amine compound, acting as a monobasic tridentate(NSN) ligand. The chemical behavior of its technetium analog has been studied radioanalytically by solvent extraction, TLC, electrophoresis and HPLC using 99mTc tracer.