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Updated: Jul 11, 2026

Preparation of Authigenic Pyrite from Methane-bearing Sediments for In Situ Sulfur Isotope Analysis Using SIMS
Published on: August 31, 2017
A method for generating uniform size-segregated pyrite particle fractions
Amy L Wolfe1, Ran Liu, Brian W Stewart
1Department of Geology and Planetary Science, University of Pittsburgh, Pittsburgh, PA 15260, USA. alw11@pitt.edu
A new wet sieving method prepares pyrite samples for dissolution experiments. This technique ensures consistent particle size distribution, improving the reliability of experimental results and comparisons.
Area of Science:
- Geochemistry
- Mineralogy
- Experimental Petrology
Background:
- Standardized sample preparation is crucial for comparing pyrite dissolution experiments across different conditions.
- Assessing dry and wet sieving methods is necessary to develop reproducible techniques for size-specific mineral analysis.
Purpose of the Study:
- To evaluate dry and wet sieving preparation methods for pyrite.
- To establish a reproducible technique for obtaining uniformly sized pyrite particles within a specific size range.
Main Methods:
- A wet sieving preparation method was developed and described.
- The method focuses on concentrating pyrite particles within the 44-75 micrometer diameter range.
- The technique inherently removes adhering particles, eliminating the need for post-processing cleanup.
Main Results:
- The wet sieving method successfully isolates pyrite particles in the 44-75 micrometer size range.
- Pyrite size distribution is significantly influenced by sample preparation methods.
- Apparent pyrite dissolution rates are affected by the chosen preparation technique.
Conclusions:
- The described wet sieving methodology is non-destructive to pyrite samples.
- This technique utilizes standard laboratory equipment and is readily accessible.
- The method has potential applicability to other minerals beyond pyrite.
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