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Separation of trace elements in solid samples by formation of volatile inorganic compounds
1Fachbereich für Anorganische Chemie und Kernchemie Technische Hochschule Darmstadt, 6100 Darmstadt, FRG.
This study reviews methods for separating and determining trace elements using volatilization and gas chromatography. It details typical separations and apparatus for inorganic gas chromatography applications.
Area of Science:
- Analytical Chemistry
- Inorganic Chemistry
Background:
- Trace element analysis is crucial in various scientific fields.
- Traditional methods for trace element determination can be complex and time-consuming.
Purpose of the Study:
- To review and consolidate methods for trace element separation and determination.
- To highlight the utility of volatilization and gas chromatography in this context.
Main Methods:
- Review of existing literature on separation techniques.
- Focus on volatilization as a pre-concentration and separation step.
- Discussion of gas chromatography principles and applications in inorganic analysis.
Main Results:
- Volatilization coupled with gas chromatography offers efficient separation of trace elements.
- Specific examples of successful separations are presented.
- Apparatus suitable for inorganic gas chromatography is described.
Conclusions:
- Gas chromatography is a powerful technique for trace element analysis.
- Volatilization enhances the applicability of gas chromatography for inorganic samples.
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