Related Experiment Video
Updated: Jun 22, 2026

Standard Test Method ASTM D 7998-19 for the Cohesive Strength Development of Wood Adhesives
Published on: May 17, 2020
Bracket bond strengths of new adhesive systems
Gerald T Minick1, Larry J Oesterle, Sheldon M Newman
1Department of Orthodontics, School of Dentistry, University of Colorado at Denver and Health Sciences Center, Aurora, CO 80045, USA.
Introduction:
Amorphous calcium phosphate, antibacterial monomer MDPB (12-methacryloyloxydodecyl-pyridinium bromide), and self-etching primers are some of the novel elements now added to bonding systems. The purpose of this study was to compare bond strengths of newer bonding systems with either bioactive components or self-etching primers with a conventional bonding system.
Methods:
Four new bonding systems, Aegis Ortho (with amorphous calcium phosphate) (Harry J. Bosworth, Skokie, Ill), Clearfil Protect Bond (self-etching primer with an antibacterial monomer) (Kuraray Dental, Kurashiki, Japan), iBond (reformulated self-etching primer) (Heraeus Kulzer, Hanau, Germany), and Clearfil S3 Bond (self-etching primer with combined hydrophilic and hydrophobic technology) (Kuraray Dental), were tested and compared with Transbond XT, a conventional bracket bonding system (3 M Unitek, Monrovia, Calif). Brackets bonded with these materials were tested in the shear-peel mode at 30 minutes and 24 hours, and the location of the bond failures was observed.
Results:
The newer bonding systems Aegis Ortho (5.3 +/- 0.5 MPa at 30 minutes, 7.2 +/- 0.7 MPa at 24 hours), Clearfil Protect Bond (7.1 +/- 0.8 MPa at 30 minutes, 6.1 +/- 0.6 MPa at 24 hours), Clearfil S3 Bond (3.8 MPa at 30 minutes, 6.6 +/- 0.5 MPa at 24 hours), and iBond (3.9 +/- 0.4 MPa at 30 minutes, 3.9 +/- 0.3 MPa at 24 hours) achieved shear bond strengths significantly lower than Transbond XT (10.1 +/- 0.8 MPa at 30 minutes, 10.1 +/- 1.0 MPa at 24 hours).
Conclusions:
Aegis Ortho, Clearfil Protect Bond, Clearfil S3 Bond, and iBond produced lower bond strengths than did Transbond XT, with iBond's strength lower than what might be acceptable for clinical usefulness.
Related Concept Videos
Bonding and Strength of Aggregate
Chemical Bonds
Atoms participate in a chemical bond formation to acquire a completed valence-shell electron configuration similar to that of the noble gas nearest to it in atomic number. Ionic, covalent, and metallic bonds are some of the important types of chemical bonds. Bond energy and bond length determine the strength of a chemical bond.
Types of Chemical Bonds
An ionic bond is formed due to electrostatic attraction between cations and anions. Often, the ions are formed by the transfer of electrons from...
Accelerators
The effectiveness of calcium chloride can...
Strength of Cement
For compressive strength tests, ASTM C 109-05 standards prescribe a cement-sand mix ratio of 1:2.75 and a water/cement ratio of 0.485 for making 2-inch cubes. These cubes are mixed, cast, and cured in saturated lime water at 23°C until testing. Flexural strength testing, outlined in ASTM C...
Mortar Properties
Brick Masonry
For thicker walls, multiple wythes are bonded together using...
