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Updated: Jun 9, 2026

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An Experimental Protocol for Femtosecond NIR/UV - XUV Pump-Probe Experiments with Free-Electron Lasers
Published on: October 23, 2018
Nanosecond x-ray Laue diffraction apparatus suitable for laser shock compression experiments
Matthew Suggit1, Giles Kimminau, James Hawreliak
1Department of Physics, Clarendon Laboratory, University of Oxford, Parks Road, Oxford OX1 3PU, United Kingdom. matthew.suggit@physics.ox.ac.uk
The Review of Scientific Instruments
|September 7, 2010
Summary
Researchers generated quasiwhite-light X-rays using laser-produced plasma for single-crystal Laue diffraction. This method enables rapid X-ray diffraction pattern capture from shocked and unshocked silicon crystals.
Area of Science:
- Materials Science
- Plasma Physics
- Crystallography
Background:
- Laue diffraction is a powerful technique for analyzing crystal structures.
- Generating suitable X-ray sources for rapid, single-shot diffraction experiments presents a challenge.
- Laser-produced plasmas offer a potential route to high-brightness X-ray sources.
Purpose of the Study:
- To develop a quasiwhite-light X-ray source for Laue diffraction.
- To demonstrate the capability of this source for single-shot diffraction from single crystals.
- To investigate the structural changes in laser-shocked silicon crystals.
Main Methods:
- Utilized nanosecond bursts of X-rays from a laser-produced plasma containing mid-Z elements.
- Generated a quasiwhite-light X-ray spectrum with energies from 3 to over 10 keV.
- Performed single-shot nanosecond Laue diffraction on unshocked and laser-shocked silicon crystals.
Main Results:
- Successfully produced a quasiwhite-light X-ray spectrum suitable for Laue diffraction.
- Recorded bright, single-shot nanosecond diffraction patterns from single crystals.
- Obtained diffraction patterns from both unshocked and shocked silicon, indicating the method's applicability to dynamic studies.
Conclusions:
- Laser-produced plasma X-rays provide a viable source for rapid Laue diffraction.
- The developed technique is suitable for studying dynamic processes like laser-induced shock in crystals.
- Single-shot diffraction captures structural information from transient states in materials.

