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Melaminium iodide monohydrate.

Min Min Zhao1, Ping Ping Shi

  • 1Ordered Matter Science Research Center, College of Chemistry and Chemical, Engineering, Southeast University, Nanjing 211189, People's Republic of China.

Acta Crystallographica. Section E, Structure Reports Online
|May 18, 2011
PubMed
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This study details the crystal structure of melaminium iodide monohydrate, revealing extensive hydrogen bonding networks. These interactions, including N-H⋯O, N-H⋯N, and O-H⋯I bonds, form interconnected ribbons and influence crystal packing.

Area of Science:

  • Crystallography
  • Materials Science
  • Supramolecular Chemistry

Background:

  • Melaminium salts are of interest due to their potential applications.
  • Understanding the hydrogen bonding in crystalline solids is crucial for predicting their properties.

Purpose of the Study:

  • To elucidate the detailed crystal structure of melaminium iodide monohydrate.
  • To identify and characterize the hydrogen bonding interactions and supramolecular assembly.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the crystal structure.
  • Analysis of hydrogen bond geometries and distances was performed.

Main Results:

  • The crystal structure of melaminium iodide monohydrate (C(3)H(7)N(6) (+)·I(-)·H(2)O) was determined.

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  • All hydrogen atoms of the melaminium cation participate in hydrogen bonding.
  • Interconnected ribbons formed by N-H⋯N and N-H⋯O hydrogen bonds along [111] were observed.
  • The ribbons are further linked by O-H⋯I and N-H⋯I hydrogen bonds and π-π interactions.

    • Conclusions:

    • The melaminium cation, iodide anion, and water molecules form a complex hydrogen-bonded network.
    • The identified hydrogen bonding patterns and π-π interactions dictate the supramolecular architecture of the crystal.