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High-speed force load in force measurement in liquid using scanning probe microscope.

Yan Zhang1, Qingze Zou

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Area of Science:

  • Soft Matter Physics
  • Materials Science
  • Nanotechnology

Background:

  • Scanning Probe Microscopy (SPM) is crucial for analyzing soft and biological materials in liquid.
  • High-speed force measurements are necessary for dynamic sample evolution and viscoelasticity studies.
  • Liquid environments present challenges including thermal drift, low signal-to-noise ratio, hydrodynamic forces, and actuator dynamics.

Purpose of the Study:

  • To develop a novel approach for high-speed, precise force loading in liquid using SPM.
  • To address and mitigate adverse effects impacting force measurements in dynamic liquid environments.
  • To enable accurate characterization of soft materials under demanding measurement conditions.

Main Methods:

  • Implementation of an inversion-based iterative feedforward-feedback (II-FF/FB) control strategy.
  • Experimental application to high-speed force-curve measurements.
  • Utilizing SPM for force-distance profiling of soft materials in aqueous media.

Main Results:

  • The II-FF/FB approach successfully achieved high-speed force loading with enhanced precision.
  • Demonstrated mitigation of thermal drift, hydrodynamic effects, and actuator dynamics.
  • Enabled accurate force measurements for dynamic analysis of soft materials in liquid.

Conclusions:

  • The developed II-FF/FB method provides a robust solution for high-speed SPM force measurements in liquid.
  • This technique is vital for interrogating the mechanical properties of soft and biological materials.
  • The approach paves the way for advanced characterization of rate-dependent viscoelasticity in dynamic environments.