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Low solvothermal synthesis and characterization of hollow nanospheres molybdenum sulfide
H Akram1, C Mateos-Pedrero, E Gallegos-Suárez
1Grupo de diseño molecular de catalizadores heterogéneos, Instituto de Catálisis y Petroleoquímica, UA UNED-ICP (CSIC), Campus de Cantoblanco, 28049 Madrid, Spain.
Journal of Nanoscience and Nanotechnology
|September 12, 2012
Abstract:
Hollow nanospheres of molybdenum disulfide have been synthesized by a novel solvothermal method under low temperature (180 degrees C). These nanomaterials were characterized by X-ray diffraction (XRD), Fourier transformation infra-red spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM, HRTEM) and X-ray Photoelectron Spectroscopy (XPS). A mechanism for the synthesis reaction is tentatively proposed and discussed.