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Updated: May 17, 2026

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Synthesis of High Purity Nonsymmetric Dialkylphosphinic Acid Extractants
Published on: October 19, 2017
N,N'-Dibenzyl-N''-(2-chloro-2,2-difluoro-acet-yl)phospho-ric triamide
Mehrdad Pourayoubi1, Mojtaba Keikha, Jerry P Jasinski
1Department of Chemistry, Ferdowsi University of Mashhad, Mashhad, Iran.
Acta Crystallographica. Section E, Structure Reports Online
|November 6, 2012
Abstract:
In the title mol-ecule, C(16)H(17)ClF(2)N(3)O(2)P, the N-H unit of the C(=O)NHP(=O) fragment adopts a syn orientation with respect to the P=O group. The two F atoms and the Cl atom of the ClF(2)C group are disordered over two sets of sites with refined occupancies of 0.605 (6) and 0.395 (6). In the crystal, mol-ecules are linked via N-H⋯O=C hydrogen bonds the and the (N-H⋯)(N-H⋯)O=P group into chains along [010].
