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Updated: May 14, 2026

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Thermal Measurement Techniques in Analytical Microfluidic Devices
Published on: June 3, 2015
Note: Focus error detection device for thermal expansion-recovery microscopy (ThERM).
1Laboratorio de Electrónica Cuántica, Departamento de Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Buenos Aires, Argentina.
The Review of Scientific Instruments
|February 8, 2013
Summary
This study introduces a novel focus error detection method for accurately measuring thermal diffusivity. The technique achieves high resolution by isolating surface curvature effects, enabling precise material property analysis.
Area of Science:
- Materials Science
- Optical Metrology
- Thermal Analysis
Background:
- Surface curvature variations can interfere with optical measurements.
- Existing methods may be affected by thermoreflectance and photodefelection.
- Accurate measurement of thermal diffusivity is crucial for material characterization.
Purpose of the Study:
- To develop a focus error detection method insensitive to thermoreflectance and photodefelection.
- To enable precise measurement of thermal diffusivity with high spatial resolution.
- To utilize an astigmatic probe laser and four-quadrant detector for surface analysis.
Main Methods:
- Implementing an astigmatic probe laser and a four-quadrant detector for focus error detection.
- Applying nonlinear curve fitting to the defocusing signal to determine a cutoff frequency.
- Isolating surface curvature variations to cancel interfering optical effects.
Main Results:
- The developed method is solely sensitive to surface curvature variations.
- A cutoff frequency dependent only on thermal diffusivity and pump beam size is retrieved.
- Microscopic lateral resolution and high axial resolution (~100 pm) are achieved.
Conclusions:
- A straightforward method for retrieving thermal diffusivity with high resolution is presented.
- The technique effectively cancels confounding thermoreflectance and photodefelection effects.
- This innovation offers precise material property analysis capabilities.

