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Related Concept Videos

Effects of EDTA on End-Point Detection Methods01:18

Effects of EDTA on End-Point Detection Methods

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Different methods, such as visual observance of metal-ion indicators, spectroscopic techniques, and potentiometric methods, can determine the endpoint of an EDTA titration.
In the visual method, metal-ion indicators (metallochromic dyes), which have distinct colors in their free and complex forms, are added to the mixture to signal the titration's end point. They form stable complexes with metal ions, but these complexes are weaker than the corresponding metal–EDTA complexes. As a...
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Comprehensive Characterization of Extended Defects in Semiconductor Materials by a Scanning Electron Microscope
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Introduction and comparison of new EBSD post-processing methodologies.

Stuart I Wright1, Matthew M Nowell1, Scott P Lindeman1

  • 1EDAX, 392 East 12300 South, Suite H, Draper, UT 84020, USA.

Ultramicroscopy
|September 7, 2015
PubMed
Summary
This summary is machine-generated.

Electron Backscatter Diffraction (EBSD) data quality can be improved using new post-processing methods. Local pattern averaging offers the most significant enhancement for noisy EBSD patterns, particularly those from camera issues.

Keywords:
EBSDElectron Backscatter Diffraction

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Area of Science:

  • Materials Science
  • Crystallography
  • Electron Microscopy

Background:

  • Electron Backscatter Diffraction (EBSD) is crucial for microstructure characterization.
  • Obtaining indexable diffraction patterns can be challenging, leading to noisy EBSD maps.
  • Existing post-processing methods correlate neighboring points to improve data quality.

Purpose of the Study:

  • To introduce and evaluate two novel post-processing techniques for improving noisy EBSD data.
  • To assess the effectiveness of these methods on artificially and operationally induced noise, as well as challenging sample types.
  • To validate indexing success rate metrics for EBSD data analysis.

Main Methods:

  • Development of a re-scanning approach utilizing local pattern averaging.
  • Implementation of a method using multiple solutions from the triplet indexing technique.
  • Application of these methods to EBSD data with introduced noise and to deformed/fine-grained samples.

Main Results:

  • Both introduced techniques improved the quality of the reconstructed EBSD scan data.
  • Local pattern averaging demonstrated the most significant improvement among the tested methods.
  • Local pattern averaging was most effective for noise originating from camera operating conditions.

Conclusions:

  • The novel post-processing techniques effectively enhance noisy EBSD datasets.
  • Local pattern averaging is a promising method, especially for camera-related noise.
  • The fraction of points with high Confidence Index (CI) values accurately reflects EBSD indexing success rates.