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A High-Temperature Transient Hot-Wire Thermal Conductivity Apparatus for Fluids.

R A Perkins1, H M Roder1, C A Nieto de Castro2

  • 1National Institute of Standards and Technology, Boulder, CO 80303.

Journal of Research of the National Institute of Standards and Technology
|February 11, 2017
PubMed
Summary
This summary is machine-generated.

A new apparatus accurately measures fluid thermal conductivity and diffusivity using a transient hot-wire technique. This instrument provides precise data for fluids like toluene, argon, and nitrogen.

Keywords:
argonheat capacitynitrogenradiation correctionthermal conductivitythermal diffusivitytoluenetransient hot-wire

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Area of Science:

  • Thermodynamics
  • Fluid dynamics
  • Materials science

Background:

  • Accurate measurement of thermophysical properties is crucial for fluid characterization.
  • Existing methods may have limitations in temperature, pressure, or accuracy.
  • Transient hot-wire techniques offer potential for precise measurements.

Purpose of the Study:

  • To develop and describe a novel apparatus for measuring thermal conductivity and diffusivity of fluids.
  • To validate the instrument's performance using well-characterized fluids.
  • To present new thermal property data for liquid toluene, including radiation effects.

Main Methods:

  • Utilizes a step-power-forced transient hot-wire technique with two platinum wires.
  • Employs a Wheatstone bridge configuration for differential measurement.
  • Automated control and data acquisition using a microcomputer.

Main Results:

  • The apparatus measures thermal conductivity and diffusivity for fluids between 220-775 K and up to 70 MPa.
  • Verified performance with measurements on liquid toluene, argon, and nitrogen.
  • Reported new, radiation-corrected thermal conductivity data for liquid toluene (±0.3% precision, ±1% accuracy).
  • Achieved ±5% accuracy for thermal diffusivity measurements.

Conclusions:

  • The developed apparatus is effective for precise thermophysical property measurements of fluids.
  • New data for liquid toluene highlight the significance of radiative heat transfer.
  • The instrument enables calculation of specific heat when density is known.