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Facile Preparation of Haggite by Reducing V2O5 in Guaiacol/Methanol Solution
Fei Yan1, Yunfei Bai1, Yushuai Sang1
1State Key Laboratory of Chemical Engineering, Tianjin Key Laboratory of Applied Catalysis Science and Technology, School of Chemical Engineering , Tianjin University and Collaborative Innovation Center of Chemical Science and Engineering , Tianjin 300072 , China.
Abstract:
Haggite-structured V4O6(OH)4 is prepared via a one-step reduction of V2O5 in a mixture of guaiacol and methanol. Guaiacol delays the overreduction of Haggite to V2O3. The time window for the stable existence of the Haggite phase is enlarged at low temperature.
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