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Updated: Feb 3, 2026

Non-invasive 3D-Visualization with Sub-micron Resolution Using Synchrotron-X-ray-tomography
Published on: May 27, 2008
On evaluating x-ray imaging crystals with synchrotron radiation.
N R Pereira1, A T Macrander2, C Stoeckl3
1Ecopulse, Inc., 7844 Vervain Ct., Springfield, Virginia 22152, USA.
Local x-ray diffraction measurements reveal crystal imperfections. A specialized quartz conditioning crystal enhances resolution, making fabrication flaws visible for improved plasma diagnostics.
Area of Science:
- Plasma diagnostics
- X-ray optics
- Materials science
Background:
- Bent crystals are used in plasma diagnostics, diffracting X-rays across the entire crystal.
- Analyzing the overall spectrum or image of diffracted X-rays is insufficient for identifying individual crystal performance issues.
Purpose of the Study:
- To develop a method for measuring X-ray diffraction locally with high resolution.
- To identify specific reasons for performance variations in bent crystals used for plasma diagnostics.
Main Methods:
- Utilized an x-ray topography setup at the Advanced Photon Source (APS) beamline 1-BM.
- Employed a specially designed quartz conditioning crystal to improve radiation quality.
Main Results:
- The new method enabled local diffraction measurements with necessary resolution.
- Standard synchrotron X-ray optics were insufficient for this task.
- Worrisome diffraction features were eliminated, and minor fabrication flaws became highly visible.
Conclusions:
- Local X-ray diffraction measurement with a specialized setup provides superior insight into bent crystal performance.
- This technique is crucial for understanding and improving crystals used in plasma diagnostics.
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