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Low-cost disposable high-pressure setup for in situ X-ray experiments
Maarten Houlleberghs1, Johan A Martens1, Eric Breynaert1
1Center for Surface Chemistry and Catalysis (COK), KU Leuven, Celestijnenlaan 200f, Box 2461, Heverlee 3001, Belgium.
Journal of Synchrotron Radiation
|November 9, 2018
Summary
Researchers developed a quick and affordable method for disposable sample cells. This technique is ideal for in situ catalytic and material synthesis studies.
Area of Science:
- Materials Science
- Chemical Engineering
- Analytical Chemistry
Background:
- In situ studies require specialized sample cells for real-time analysis.
- Existing methods for fabricating sample cells can be costly and time-consuming.
Purpose of the Study:
- To present a low-cost, flexible, and rapid method for creating disposable sample cells.
- To enable in situ catalytic and material synthesis studies.
Main Methods:
- Utilizing standard quartz capillaries.
- Employing heat-shrinkable tubing for sealing and assembly.
- Incorporating standard Swagelok components for robust connections.
Main Results:
- Successfully fabricated functional disposable sample cells.
- Demonstrated suitability for in situ catalytic and material synthesis applications.
- Method proved to be cost-effective, flexible, and fast.
Conclusions:
- The described method offers an accessible approach to fabricating disposable sample cells.
- This technique facilitates advanced in situ investigations in catalysis and materials science.
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