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Updated: Dec 21, 2025

High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
Published on: October 9, 2020
Combining high temperature sample preparation and in-situ magnetic fields in XPEEM
Anna Mandziak1, Juan de la Figuera2, Jose Emilio Prieto2
1Alba Synchrotron Light Facility, CELLS, Barcelona E-08290, Spain; Instituto de Química Física 'Rocasolano', Madrid E-28006, Spain.
Abstract:
We present a custom-made sample holder system for use in Elmitec Low Energy and PhotoEmission Electron Microscopes. It consists of two different sample holder bodies: one with a filament for high temperature measurements (up to more than 1500 K) and the other with integrated electromagnets for the in-situ application of in-plane/out-of-plane small magnetic fields. The sample is placed on a platelet which can be transferred between the two holders. This opens up new possibilities for the preparation of samples at high temperatures and investigation of their behavior under applied magnetic fields without leaving the ultra high vacuum system.

