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High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
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Decoherence optimized tilted-angle cross polarization: A novel concept for sensitivity-enhanced solid-state NMR using

Tatsuya Matsunaga1, Isamu Matsuda2, Toshio Yamazaki1

  • 1NMR Division, the RIKEN SPring-8 Center, RIKEN, 1-7-22 Suehiro-cho, Tsurumi-ku, Yokohama, Kanagawa 230-0045, Japan.

Journal of Magnetic Resonance (San Diego, Calif. : 1997)
|November 23, 2020
PubMed
Summary

Ultra-fast magic-angle spinning solid-state NMR (SSNMR) is enhanced by a new decoherence-optimized tilted-angle cross-polarization (DOTA CP) method. DOTA CP improves sensitivity and polarization transfer for rare spins like carbon-13.

Keywords:
(1)H-detected solid-state NMRBiomolecular NMRCPMulti-dimensional solid-state NMRSolid state NMRUltra-fast MAS

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