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Atomic Force Microscopy Cantilever-Based Nanoindentation: Mechanical Property Measurements at the Nanoscale in Air and Fluid
Published on: December 2, 2022
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Wear comparison of critical dimension-atomic force microscopy tips
Ndubuisi G Orji1, Ronald G Dixson1, Ernesto Lopez2
1National Institute of Standards and Technology, Gaithersburg, MD 20850, USA.
Summary
Electron beam deposited tips significantly reduce wear and extend lifetime for critical dimension atomic force microscopy (CD-AFM), improving measurement accuracy and lowering costs.
Area of Science:
- Materials Science
- Nanotechnology
- Metrology
Background:
- Nanoscale wear impacts atomic force microscopy (AFM) measurements across various applications, including process control and nanoelectronics.
- Reducing AFM tip wear is crucial for maintaining measurement accuracy and reliability.
- Limited research exists on tip wear specifically for critical dimension AFM (CD-AFM), despite its direct effect on dimensional measurements.
Purpose of the Study:
- To investigate the wear performance of electron beam deposited (EBD) CD-AFM tips.
- To compare the wear rate and tip lifetime of EBD tips against conventional silicon-based CD-AFM tips.
- To understand the fundamental aspects of CD-AFM tip wear to enhance measurement accuracy.
Main Methods:
- Utilized a continuous scanning strategy to evaluate tip wear.
- Quantified wear rates and determined tip lifetimes for EBD CD-AFM tips.
- Performed comparative analysis with silicon-based CD-AFM tips.
Main Results:
- Electron beam deposited CD-AFM tips demonstrated a tip lifetime improvement of up to five times compared to silicon tips.
- Wear rates for EBD tips were reduced by more than 17 times.
- These findings indicate significantly enhanced durability and reduced degradation of EBD tips.
Conclusions:
- Electron beam deposited tips offer a substantial improvement in wear resistance for CD-AFM applications.
- Reduced wear rates translate to decreased measurement variability and potentially lower operational costs.
- The study provides essential insights into CD-AFM tip wear, paving the way for more robust nanoscale metrology.

