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Microplastics: An overview on separation, identification and characterization of microplastics
Anita Tirkey1, Lata Sheo Bachan Upadhyay1
1National Institute of Technology Raipur, Department of Biotechnology, Raipur, Chhattisgarh 492010, India.
Marine Pollution Bulletin
|June 19, 2021
Summary
Plastic residues, including microplastics (<5 mm) and nanoplastics (<1 μm), pose environmental threats. This review covers sampling and identification methods for these pervasive plastic pollutants.
Area of Science:
- Environmental Science
- Analytical Chemistry
- Materials Science
Background:
- Plastic residues are a significant environmental threat.
- Microplastics (<5 mm) and nanoplastics (<1 μm) are pervasive and difficult to remove.
- Their small size complicates detection and remediation efforts.
Purpose of the Study:
- To provide an overview of microplastic concerns.
- To review current methods for microplastic sampling and identification.
- To identify areas for future technological development.
Main Methods:
- Sampling techniques discussed include sieving, filtration, visual sorting, digestion, and density separation.
- Identification methods covered are Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEM-EDS), Fourier-Transform Infrared Spectroscopy (FTIR), Near-Infrared Spectroscopy (NIR), Raman Spectroscopy, and Nuclear Magnetic Resonance (NMR) Spectroscopy.
- The review synthesizes information on established and emerging analytical approaches.
Main Results:
- Various methods exist for microplastic sampling and identification in environmental matrices.
- Current techniques provide valuable data but have limitations in terms of cost and portability.
- The review highlights the effectiveness of techniques like SEM-EDS and FTIR for microplastic characterization.
Conclusions:
- Effective sampling and identification are crucial for understanding microplastic pollution.
- There is a need for more economical and portable techniques for microplastic analysis.
- Further research and development are required to address the challenges posed by microplastics and nanoplastics.

