Related Experiment Video
Updated: Oct 16, 2025

In situ Grazing Incidence Small Angle X-ray Scattering on Roll-To-Roll Coating of Organic Solar Cells with Laboratory X-ray Instrumentation
Published on: March 2, 2021
Grazing-incidence X-ray diffraction tomography for characterizing organic thin films.
Esther H R Tsai1, Yu Xia2, Masafumi Fukuto3
1Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, NY 11973, USA.
Grazing-incidence diffraction tomography (GID tomography) quantitatively analyzes crystalline domains in thin films. This advanced X-ray technique enhances material characterization without beam coherence or substrate limitations.
Area of Science:
- Materials Science
- Crystallography
- X-ray Physics
Background:
- Accurate thin film characterization is crucial for understanding material properties and processing.
- Existing methods often have limitations regarding substrate type, film thickness, or beam coherence.
Purpose of the Study:
- To introduce a novel technique, grazing-incidence diffraction tomography (GID tomography).
- To enable quantitative determination of crystalline domain dimensions and orientation in thin films.
- To overcome limitations of current characterization methods.
Main Methods:
- Combines grazing-incidence X-ray scattering with computed tomography.
- A computational method applicable to standard X-ray scattering setups.
- Extends the capabilities of synchrotron beamlines.
Main Results:
- Quantitative determination of crystalline domain dimension and orientation.
- Applicable to various substrates and film thicknesses.
- No restrictions on beam coherence required.
Conclusions:
- GID tomography offers a versatile and powerful approach for thin film analysis.
- Enhances the utility of existing synchrotron facilities.
- Facilitates deeper understanding of structure-property relationships in thin films.
More Related Videos
06:05Using Neutron Spin Echo Resolved Grazing Incidence Scattering to Investigate Organic Solar Cell Materials
Published on: January 15, 2014
11:48Microfluidic Chips for In Situ Crystal X-ray Diffraction and In Situ Dynamic Light Scattering for Serial Crystallography
Published on: April 24, 2018
Related Concept Videos
X-ray Diffraction of Biological Samples
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are scattered by the electron clouds around the sample atoms. The X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal...
X-ray Crystallography
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...