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A simplified rapid-quench multi-anvil technique.

Dmitry Bondar1, Hongzhan Fei1, Anthony C Withers1

  • 1Bayerisches Geoinstitut, University of Bayreuth, Universitätsstraße 30, 95447 Bayreuth, Germany.

The Review of Scientific Instruments
|December 2, 2021
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Summary
This summary is machine-generated.

A new rapid-quench technique for multi-anvil presses enables routine glass formation from low glass-forming ability melts. This improved design offers better temperature stability and higher cooling rates, crucial for materials science research.

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Area of Science:

  • High-pressure experimental techniques
  • Materials science
  • Geophysics

Background:

  • Kawai-type multi-anvil presses are essential for high-pressure research.
  • Rapid-quenching is critical for preserving high-pressure phases and forming glasses.
  • Previous designs had limitations in cooling rate and ease of assembly.

Purpose of the Study:

  • To report a new, improved rapid-quench technique for Kawai-type multi-anvil presses.
  • To enhance the ability to form glasses from melts with low glass-forming ability.
  • To characterize the performance and limitations of the new rapid-quench design.

Main Methods:

  • Implementation of 3D-printed parts for coolant delivery.
  • Modification of inner anvils for enhanced coolant circulation.
  • Pressure calibration and temperature distribution analysis within the experimental cell.

Main Results:

  • The new design achieves higher cooling rates (up to 8200 °C/s) and better temperature stability.
  • Cooling rate is dependent on pressure and temperature, increasing with pressure and decreasing with temperature.
  • A significant improvement of over 15% in cooling rate compared to the previous design was achieved.
  • Pressure calibration revealed that the initial 0.6 MN press load is used to overcome tungsten component resistance.

Conclusions:

  • The upgraded rapid-quench technique facilitates routine glass formation, expanding research possibilities.
  • The pressure and temperature dependencies of the cooling rate are quantified, allowing for optimized experimental conditions.
  • The novel design allows for routine access to 9 GPa and 2200 K with minimal temperature variation, advancing high-pressure research capabilities.