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Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules

Fully Autonomous Characterization and Data Collection from Crystals of Biological Macromolecules

Published on: March 22, 2019

Towards a dynamic compression facility at the ESRF.

Nicolas Sévelin-Radiguet¹, Raffaella Torchio¹, Gilles Berruyer¹

¹European Synchrotron Radiation Facility, 71 Avenue des Martyrs, CS 40220, 38043 Grenoble, France.

Journal of Synchrotron Radiation

|January 5, 2022

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High Power Laser Facility experiments at ESRF

Area of Science:

Materials Science
Condensed Matter Physics
High-Energy Physics

Background:

The European Synchrotron Radiation Facility (ESRF) commissioned a new High Power Laser Facility.
This facility was integrated with the Energy-dispersive X-ray Absorption Spectroscopy (ED-XAS) beamline ID24.

Purpose of the Study:

To present results from the 2018 commissioning and experimental campaigns.
To demonstrate the capability of laser-driven dynamic compression experiments.

Main Methods:

Interfacing the High Power Laser Facility's front-end (15 J in 10 ns) to the ID24 beamline.
Performing online time-resolved X-ray Absorption Spectroscopy (XAS) on samples under dynamic compression.

Main Results:

Keywords:

dynamic compression laser shock time-resolved XAS

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Successful commissioning and operation of the laser-beamline interface.

Acquisition of time-resolved XAS data during laser-driven dynamic compression of iron oxides, iron alloys, and bismuth.

Conclusions:

The integrated system enables novel dynamic compression studies.
The facility is ready for advanced research in materials under extreme conditions.