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Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

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Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
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    Area of Science:

    • Optics and Photonics
    • Materials Science
    • Physical Chemistry

    Background:

    • Previous work introduced an infrared laser ellipsometer for spectroscopy and hyperspectral imaging.
    • Further development was needed for faster, more sensitive thin-film measurements.

    Purpose of the Study:

    • To report on a next-generation multi-timescale ellipsometer.
    • To achieve high time resolution (10 µs) and spectral resolution (0.2 cm⁻¹) for simultaneous amplitude and phase measurements.
    • To investigate the dynamics of fatty acid thin-film formation.

    Main Methods:

    • Development of a multi-timescale ellipsometer.
    • Spectroscopic analysis of thin-film formation from evaporating microliter droplets.
    • Probing optical thickness, structure, and molecular interactions during phase transitions.

    Main Results:

    • Achieved 10 µs time resolution and long-term stability over hours.
    • Demonstrated high spectral resolution of 0.2 cm⁻¹.
    • Investigated temporal stages (milliseconds to minutes) of fatty acid thin-film formation.

    Conclusions:

    • The multi-timescale ellipsometer provides unprecedented temporal resolution for thin-film analysis.
    • This technique can monitor optical thickness, structural changes, and molecular interactions during phase transitions.
    • Potential applications include in situ biosensing, microfluidics, polymer analytics, and operando studies.