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Developing Core/Shell Capsules Based on Hydroxypropyl Methylcellulose and Gelatin through Electrodynamic Atomization
Carol López de Dicastillo1, Eliezer Velásquez2,3, Adrián Rojas2,3
1Packaging Laboratory, Institute of Agrochemistry and Food Technology (IATA-CSIC), Av. Agustín Escardino 7, 46980 Paterna, Spain.
Polymers
|January 21, 2023
Summary
Encapsulating beetroot betalains using coaxial electrospraying with gelatin and hydroxypropyl methylcellulose enhances their stability. The core-shell structure with gelatin in the core and HPMC in the shell offers superior betalain protection for food applications.
Area of Science:
- Food Science and Technology
- Biomaterials Engineering
- Nutraceutical Chemistry
Background:
- Betalains, natural pigments from beetroot, offer health benefits but are unstable.
- Their sensitivity to external factors limits their application in food products.
- Efficient encapsulation is crucial for preserving betalain bioactivity and color.
Purpose of the Study:
- To develop and evaluate a core-shell encapsulation system for beetroot betalains.
- To investigate the protective effects of different polymeric matrices (gelatin and HPMC) in core-shell structures.
- To optimize encapsulation for enhanced stability and potential food applications.
Main Methods:
- Extraction and quantification of betacyanin and betaxanthin from red beetroot.
- Coaxial electrospraying to create core-shell capsules using hydroxypropyl methylcellulose (HPMC) and gelatin (G).
- Analysis of morphological, optical, structural, thermogravimetric properties, and encapsulation efficiency.
Main Results:
- Successful encapsulation of beetroot betalains into HPMC/G core-shell structures.
- The core-shell structure with gelatin in the core and HPMC in the shell demonstrated superior betalain protection.
- Thermogravimetric and encapsulation efficiency analyses confirmed enhanced stability in the optimized structure.
Conclusions:
- The developed core-shell electrosprayed capsules effectively protect sensitive beetroot betalains.
- The specific arrangement of gelatin and HPMC is key to achieving high encapsulation efficiency and stability.
- This encapsulation strategy shows significant promise for incorporating stable betalains into food products.

