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Related Experiment Video

Updated: Aug 4, 2025

Layer-by-layer Synthesis and Transfer of Freestanding Conjugated Microporous Polymer Nanomembranes
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Layer-by-layer Synthesis and Transfer of Freestanding Conjugated Microporous Polymer Nanomembranes

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A general synthetic method towards conjugated microporous polymers with ordered bicontinuous mesostructures.

Qiqi Yang1, Yamei Liu1, Luoxing Xiang1

  • 1School of Chemistry and Chemical Engineering, Frontiers Science Center for Transformative Molecules, Shanghai Key Laboratory of Electrical Insulation and Thermal Ageing, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, China. mai@sjtu.edu.cn.

Chemical Communications (Cambridge, England)
|April 3, 2023
PubMed
Summary

Researchers developed a universal method using block copolymer self-assembly to create novel conjugated microporous polymers (CMPs) with bicontinuous structures. This work introduces new topologies for porous materials, expanding the possibilities for CMP synthesis.

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Area of Science:

  • Materials Science
  • Polymer Chemistry
  • Nanotechnology

Background:

  • Conjugated microporous polymers (CMPs) are advanced materials with tunable electronic and porous properties.
  • Synthesizing CMPs with specific, ordered mesostructures like bicontinuous networks remains a significant challenge.
  • Existing methods often lack universality and control over complex polymer topologies.

Purpose of the Study:

  • To establish a universal self-assembly approach for synthesizing novel CMPs.
  • To create CMPs exhibiting bicontinuous mesostructures.
  • To explore new synthetic routes for CMPs with diverse and complex topologies.

Main Methods:

  • Utilized block copolymer self-assembly as a templating strategy.
  • Synthesized three novel hexaazatriphenylene (Aza)-fused CMPs (Aza-CMPs).
  • Characterized the resulting polymers for their structural and morphological properties.

Main Results:

  • Successfully demonstrated a universal method for CMP synthesis via block copolymer self-assembly.
  • Achieved bicontinuous mesostructures in the synthesized Aza-CMPs.
  • Synthesized Aza-CMPs with well-defined double diamond topologies.

Conclusions:

  • The block copolymer self-assembly approach provides a versatile route to novel CMPs.
  • This method enables the creation of CMPs with intricate bicontinuous and double diamond structures.
  • The study expands the library of accessible porous materials and offers new synthetic pathways for advanced polymer architectures.