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Related Experiment Video

Updated: Jun 7, 2026

Probing and Mapping Electrode Surfaces in Solid Oxide Fuel Cells

Probing and Mapping Electrode Surfaces in Solid Oxide Fuel Cells

Published on: September 20, 2012

Localised degradation within sulfide-based all-solid-state electrodes visualised by Raman mapping.

Jungwoo Lim^1,2, Yundong Zhou^1,2, Rory H Powell^1,2

¹Stephenson Institute for Renewable Energy, Department of Chemistry, University of Liverpool, Liverpool L69 7ZF, UK. hardwick@liverpool.ac.uk.

Chemical Communications (Cambridge, England)

|June 7, 2023

Summary

This summary is machine-generated.

Degradation products form in solid electrolytes like beta-Li3PS4 after initial cycling. Raman microscopy mapped these side reactions at the cathode particle interface in sulfide solid-state batteries.

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Last Updated: Jun 7, 2026

Probing and Mapping Electrode Surfaces in Solid Oxide Fuel Cells

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Elemental-sensitive Detection of the Chemistry in Batteries through Soft X-ray Absorption Spectroscopy and Resonant Inelastic X-ray Scattering

Elemental-sensitive Detection of the Chemistry in Batteries through Soft X-ray Absorption Spectroscopy and Resonant Inelastic X-ray Scattering

Published on: April 17, 2018

Area of Science:

Materials Science
Electrochemistry
Solid-State Batteries

Background:

Sulfide solid electrolytes are promising for next-generation batteries.
Understanding degradation mechanisms is crucial for improving battery performance and lifespan.
Composite electrodes are commonly used in solid-state battery designs.

Purpose of the Study:

To map the distribution of degradation products in common sulfide solid electrolytes.
To investigate the location and nature of side reactions occurring during battery cycling.
To understand the interfacial chemistry between solid electrolytes and cathode materials.

Main Methods:

Raman microscopy was employed to analyze the chemical composition and spatial distribution of materials.
The study examined three types of sulfide solid electrolytes: beta-Li3PS4, Li6PS5Cl, and Li10GeP2S12.
Composite electrodes containing LiNi0.6Mn0.2Co0.2O2 were subjected to charge-discharge cycling.

Main Results:

Degradation products were observed in all composite electrodes after the first charge-discharge cycle.
These side reaction products were localized at the interface with the LiNi0.6Mn0.2Co0.2O2 cathode particles.
The distribution of degradation products within the sulfide electrolytes was successfully mapped.

Conclusions:

Initial cycling in sulfide solid-state batteries leads to the formation of degradation products.
These degradation products are primarily located at the cathode-electrolyte interface.
Further research is needed to mitigate these side reactions and enhance battery stability.