Analytical Models for Grain Size Determination of Metallic Coatings and Machined Surface Layers Using the Four-Point
Thomas Mehner1, Thomas Lampke1
1Materials and Surface Engineering, Institute of Materials Science and Engineering, Chemnitz University of Technology, Erfenschlager Str. 73, D-09125 Chemnitz, Germany.
Materials (Basel, Switzerland)
|September 9, 2023
Summary
Measuring electrical resistance with the four-point probe method allows for quick, non-destructive determination of metallic coating and machined surface layer grain sizes, crucial for quality control.
Area of Science:
- Materials Science
- Surface Engineering
- Corrosion Science
Background:
- Metallic coating and surface layer grain size significantly influences material properties like corrosion resistance, wear, and fatigue.
- Accurate characterization of grain size is vital for predicting and ensuring material performance in various applications.
Purpose of the Study:
- To develop a rapid, non-destructive method for determining the grain size of metallic coatings and machined surfaces.
- To establish analytical models correlating electrical resistance measurements with grain size for different grain shapes.
Main Methods:
- Utilizing the four-point probe method to measure the combined electrical resistance of the surface layer and substrate.
- Deriving analytical models based on the measured electrical resistance and considering various grain shapes.
- Employing calibration measurements to determine model parameters accurately.
Main Results:
- A non-destructive technique for determining grain size was successfully developed.
- Analytical models were established to relate electrical resistance to grain size for different grain morphologies.
- The method allows for quick and efficient grain size assessment.
Conclusions:
- The four-point probe method offers a fast and non-destructive approach to assess grain size in metallic coatings and machined surfaces.
- This technique is suitable for industrial quality control, ensuring consistent surface layer properties.
- Accurate grain size determination enhances the prediction of corrosion, wear, and fatigue behavior.
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