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Fed-batch treatment attenuates diffusional limitation while preparing high solid microfibrillated cellulose from

Nur Istianah1, Hye Jee Kang2, Sudarminto Setyo Yuwono3

  • 1School of Food Science and Biotechnology, Kyungpook National University, Daegu 41566, Republic of Korea; Department of Food Science and Biotechnology, Universitas Brawijaya, Malang 65145, Indonesia.

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Fed-batch treatment offers a promising method for producing high-solid microfibrillated cellulose (MFC) from Gelidium amansii. This approach significantly reduces energy consumption while maintaining desirable product properties, enhancing techno-economic viability.

Keywords:
NanocellulosePower consumptionProcess optimizationRed agarSemicontinuous milling

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Area of Science:

  • Materials Science
  • Biotechnology
  • Chemical Engineering

Background:

  • Microfibrillated cellulose (MFC) production often faces challenges with low solid loading and high energy consumption.
  • Gelidium amansii is a potential source for MFC, but efficient processing is key.

Purpose of the Study:

  • To investigate the impact of fed-batch treatment on the fibrillation degree and properties of Gelidium amansii-derived MFC.
  • To evaluate the techno-economic feasibility of fed-batch processing for MFC production.

Main Methods:

  • Fed-batch milling was employed, starting with 1% solid loading and progressively increasing to 5% w/v.
  • Comparison of fed-batch milling with traditional batch milling regarding solid loading, power consumption, and MFC properties.

Main Results:

  • Fed-batch processing achieved a high solid loading of approximately 10% MFC, significantly higher than batch milling's 4%.
  • Power consumption was reduced by approximately 83% compared to batch milling at 4% solid loading.
  • MFC produced via fed-batch (5% solid loading) exhibited shorter fibril length and width but a higher consistency index than MFC produced via batch milling (1% solid loading).
  • Crystallinity and decomposition temperatures remained comparable between the two methods.

Conclusions:

  • Fed-batch treatment is a viable and energy-efficient method for producing high-solid MFC from Gelidium amansii.
  • This approach offers significant techno-economic advantages for industrial MFC production without compromising key material properties.