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Related Concept Videos

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

202
Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used....
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Atomic Emission Spectroscopy: Instrumentation01:22

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The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
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Quantifying X-Ray Fluorescence Data Using MAPS
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Machine learning based unfolding of x-ray spectra from filter stack spectrometer data.

M Alvarado Alvarez1, B T Wolfe1, C-S Wong1

  • 1Los Alamos National Laboratory, Los Alamos, New Mexico 87545, USA.

The Review of Scientific Instruments
|August 1, 2024
PubMed
Summary
This summary is machine-generated.

Neural networks accurately unfold X-ray spectra from filter stack spectrometers. This method shows robustness to errors and potential for high-repetition-rate applications.

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Area of Science:

  • Spectroscopy
  • Machine Learning
  • X-ray Physics

Background:

  • Filter stack spectrometers measure X-ray energy deposition via photo-stimulated luminescence (PSL).
  • Accurate X-ray spectra unfolding is crucial for various scientific and industrial applications.

Purpose of the Study:

  • To apply neural networks for X-ray spectra unfolding using filter stack spectrometer data.
  • To evaluate the accuracy, robustness, and speed of the neural network approach.

Main Methods:

  • Training a neural network on synthetic X-ray data (<1 MeV) with Maxwellian and Gaussian distributions.
  • Utilizing PSL measurements from five distinct filter stack spectrometer designs.
  • Testing the network's performance against ground truth spectra and simulated experimental errors.

Main Results:

  • Neural network predictions closely matched ground truth spectra for single distributions, with <20% difference at high energies.
  • The network demonstrated robustness to experimental errors (<5%) and some ability to unfold mixed distributions.
  • Unfolding rates exceeded 1 Hz, suitable for high-repetition-rate systems.

Conclusions:

  • Neural networks offer a powerful and efficient tool for X-ray spectra unfolding with filter stack spectrometers.
  • The developed method is accurate, robust to experimental noise, and fast enough for demanding applications.