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Updated: May 3, 2026

Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis
Published on: December 16, 2013
Synthesis and Characterization of Porous Hydrophobic and Hydrophilic Silica Microcapsules for Applications in
Yeela Elbaz1, Taly Iline-Vul1, Aviv Dombrovsky2
1Bar-Ilan Institute of Nanotechnology and Advanced Materials (BINA), Department of Chemistry, Bar-Ilan University, Ramat-Gan 5290002, Israel.
Abstract:
Silica (SiO2) particles are widely used in various industries due to their chemical inertness, thermal stability, and wear resistance. The present study describes the preparation and potential use of porous hydrophobic and hydrophilic SiO2 microcapsules (MCs) of a narrow size distribution. First, various layers of SiO2 micro/nano-particles (M/NPs) were grafted onto monodispersed polystyrene (PS) microspheres of a narrow size distribution. Hydrophobic and hydrophilic sintered SiO2 MCs were then prepared by removing the core PS from the PS/SiO2 core-shell microspheres by burning off under normal atmospheric conditions or organic solvent dissolution, respectively. We examined how the size and quantity of the SiO2 M/NPs influence the MC's properties. Additionally, we utilized two forms of hollow SiO2 MC for different applications; one form was incorporated into polymer films, and the other was free-floating. The hydrophobic microcapsules filled with 6% hydrogen peroxide were effective in killing the tomato brown rugose fruit virus (ToBRFV). The hydrophilic microcapsules filled with thymol and thin coated onto polypropylene films were successfully used to prevent mold formation for hay protection.
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