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Sn(SO4)2·2H2O from synchrotron powder data.

Øystein Slagtern Fjellvåg1, Helmer Fjellvåg2

  • 1Institute for Energy Technology, Department Hydrogen Technology PO Box 40 NO-2027 Kjeller Norway.

Iucrdata
|January 8, 2025
PubMed
Summary

Tin(IV) sulfate dihydrate was synthesized and its crystal structure analyzed. The structure features layered octahedra connected by sulfate tetrahedra, stabilized by hydrogen bonds.

Keywords:
Sn(IV)crystal structurespowder diffractiontin(IV) sulfate dihydrate

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Area of Science:

  • Inorganic Chemistry
  • Crystallography
  • Materials Science

Background:

  • Tin(IV) sulfate dihydrate (Sn(SO4)2·2H2O) is a compound with potential applications in various chemical processes.
  • Understanding its precise crystal structure is crucial for predicting and optimizing its properties.

Purpose of the Study:

  • To synthesize tin(IV) sulfate dihydrate under specific conditions.
  • To determine the detailed crystal structure of tin(IV) sulfate dihydrate.
  • To elucidate the bonding and structural motifs within the compound.

Main Methods:

  • Synthesis via reflux in sulfuric acid under oxidizing conditions.
  • Crystal structure determination using powder synchrotron X-ray diffraction data.

Main Results:

  • The crystal structure is characterized by (100) layers of [SnO4(H2O)2] octahedra.
  • These octahedra are corner-connected by sulfate tetrahedra.
  • Moderate hydrogen bonds between water molecules and sulfate oxygen atoms stabilize the layered structure.

Conclusions:

  • The study successfully determined the crystal structure of tin(IV) sulfate dihydrate.
  • The layered structure, stabilized by hydrogen bonds, provides insights into the compound's chemical behavior.
  • This detailed structural information is valuable for further research and potential applications of tin(IV) sulfate dihydrate.