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Using Neutron Spin Echo Resolved Grazing Incidence Scattering to Investigate Organic Solar Cell Materials
Published on: January 15, 2014
Detector development for spin-echo SANS techniques using ZnS:Ag/6LiF and 6Li glass scintillators.
Giacomo Mauri1, G Jeff Sykora2, Gregory N Smith2
1Science and Technology Facilities Council, ISIS Neutron and Muon Source, Rutherford Appleton Laboratory, Didcot, Oxfordshire, OX11 0QX, UK. giacomo.mauri@stfc.ac.uk.
Neutron spin-echo techniques extend material structure analysis to larger length scales. New detectors for spin-echo modulated SANS and spin-echo SANS enhance measurement capabilities.
Area of Science:
- Materials Science
- Condensed Matter Physics
- Neutron Scattering
Background:
- Neutron spin-echo (NSE) techniques utilize Larmor precession for enhanced momentum transfer (Q) and energy (E) range in neutron scattering.
- Standard small-angle neutron scattering (SANS) is limited to 10-200 nm length scales, while NSE extends this to tens of micrometers.
Purpose of the Study:
- To present the development and performance of two novel detectors for the Larmor instrument at ISIS.
- To enable advanced neutron scattering measurements in spin-echo modulated SANS (SEMSANS) and spin-echo SANS (SESANS) modes.
Main Methods:
- Development of a ZnS:Ag/⁶LiF scintillator detector with wavelength shifting fibers (WLSF) for both SEMSANS and SESANS.
- Development of a GS20 glass scintillator detector coupled to a multi-anode photomultiplier for SESANS at higher neutron fluxes.
Main Results:
- Both detectors were successfully implemented and tested on the Larmor instrument.
- The WLSF detector and the pixelated GS20 detector demonstrated suitability for SEMSANS and SESANS applications, respectively.
Conclusions:
- The developed detectors significantly enhance the capabilities of neutron scattering instruments for studying material structures.
- Future improvements and alternative development routes show strong potential for advancing SEMSANS and SESANS applications.
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