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Enabling the Acquisition of Electron Beam-Induced Current (EBIC) Images in Conventional SEM and STEM Instruments
Fernando Camino1, Byeongjun Gil2,3, Armando Rúa4
1Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, NY 11973, USA.
This study details implementing electron beam-induced current (EBIC) imaging in scanning electron microscopes (SEM) and scanning transmission electron microscopes (STEM). It provides guidance on EBIC mechanisms and configurations for analyzing electronic materials.
Area of Science:
- Materials Science
- Physics
- Electrical Engineering
Background:
- Electron beam-induced current (EBIC) imaging is a standard technique for analyzing microelectronic devices using scanning electron microscopes (SEM).
- Recent advancements enable EBIC in aberration-corrected scanning transmission electron microscopes (STEM), allowing correlation of electronic properties with atomic structure and elemental data.
Purpose of the Study:
- To present practical methods for implementing EBIC imaging in conventional SEM and STEM systems.
- To describe the integration of lock-in EBIC with fast beam blankers.
- To elucidate the mechanisms influencing EBIC imaging and their dependencies.
Main Methods:
- Implementation of EBIC using inherent instrument electronics and third-party systems.
- Description of lock-in EBIC setup with fast beam blankers.
- Systematic investigation of EBIC mechanisms under varying beam energies, sample impedances, and electrical configurations.
Main Results:
- Demonstrated two distinct approaches for EBIC implementation in SEM and STEM.
- Detailed the lock-in EBIC technique for enhanced signal detection.
- Illustrated the impact of experimental parameters on EBIC signal generation and interpretation.
Conclusions:
- Provides researchers with foundational knowledge for applying EBIC in diverse electron microscopy setups.
- Highlights the potential of advanced EBIC techniques for in situ electronic material characterization.
- Offers practical insights into optimizing EBIC experiments for reliable analysis of charge transport properties.
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