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Updated: Apr 11, 2026

Cryogenic Sample Loading into a Magic Angle Spinning Nuclear Magnetic Resonance Spectrometer that Preserves Cellular Viability
Published on: September 1, 2020
A cryogenic probe for in situ delivery of gaseous samples for neutron scattering
Chris Baldwin1, Larissa Lopes Cavalcante2, Nicholas D Stapleton3
1Australian Nuclear Science and Technology Organisation, Locked Bag 2001, Kirrawee DC 2232, Australia.
Abstract:
This laboratory note describes an optimized solution for the delivery of gaseous samples for neutron scattering measurements. The original design to accomplish this, though effective, was not ideal from a use and maintenance perspective - especially in view of the time-constrained nature of neutron scattering experiments. In response to user demand and a need for a more reliable solution the gas-delivery sticks have been significantly redesigned, with a number of innovations applied. Here we describe the resulting equipment and the operation of the gas sticks for condensation experiments, and we present results using this equipment and methodology.

