Related Experiment Video
Updated: Jun 18, 2026

Sample Preparation and Transfer Protocol for In-Vacuum Long-Wavelength Crystallography on Beamline I23 at Diamond Light Source
Published on: April 23, 2021
High-flux, moderate-bandwidth, high-energy X-rays from lapped Si(111) crystals in a double-crystal monochromator
Hiroshi Yamazaki1,2, Kazuhiko Tahara1, Yasuhiro Shimizu1
1Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo, Hyogo 679-5198, Japan.
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Lapping the surfaces of Si(111) crystals in a double-crystal monochromator significantly increases the intensity of high-energy X-ray beams. Systematic characterization using 100 keV X-rays shows that the total flux increases by factors of 7-11 relative to polished crystals. The resulting energy bandwidth (0.12-0.21%) remains substantially narrower than that of multilayer optics. These characteristics provide a useful compromise between spectral selectivity and beam intensity, enabling practical X-ray measurements that are difficult to achieve with either perfect-crystal monochromators or multilayer optics alone. Demonstrations of imaging, powder diffraction, and incoherent micro-focusing further highlight the practical utility of the resulting beams in applications where high photon statistics are prioritized. These results demonstrate that lapped Si crystals provide a robust and cost-effective approach to generating high-flux, moderate-bandwidth high-energy X-ray beams.

