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Determining hydrogen-bond strengths in the solid state by NMR: the quantitative measurement of homonuclear J
S P Brown1, M Pérez-Torralba, D Sanz
1Laboratoire de Stéréochimie et des Interactions Moléculaires, UMR 5532 CNRS/ENS, Ecole Normale Supérieure de Lyon, 69364 Lyon, France.
Chemical Communications (Cambridge, England)
|September 26, 2002
Abstract:
Hydrogen-bonding strengths in the solid state are quantitatively determined by the accurate measurement of 15N-15N J couplings using a straightforward 2D MAS NMR spinecho approach.