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Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
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The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.

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Design and Characterization of X-Ray Multilayer Analyzers for the 50-1000 eV Region.

B L Henke1, E M Gullikson, J Kerner

  • 1Center for X-Ray Optics, Accelerator and Fusion Research Division, Lawrence Berkeley Laboratory, 1 Cyclotron Road, Berkeley, California 94720.

Journal of X-Ray Science and Technology
|February 11, 2011
PubMed
Summary
This summary is machine-generated.

This study details over a decade of developing multilayer analyzers for precise low-energy X-ray spectrometry. These advanced multilayer optics enable accurate characterization of intense X-ray sources like synchrotrons.

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Area of Science:

  • X-ray optics and instrumentation
  • Materials science for layered structures
  • Spectrometry and spectroscopy

Background:

  • Multilayer analyzers are crucial for characterizing novel intense X-ray sources.
  • Previous applications primarily focused on diagnostics and analysis.
  • A need existed for precise, absolute measurements in the low-energy X-ray range.

Purpose of the Study:

  • To present a decade of development and application of multilayer analyzers for absolute Bragg spectrometry.
  • To establish design requirements for accurate low-energy X-ray spectrometry.
  • To develop and validate analytical models for multilayer reflectivity.

Main Methods:

  • Characterization of multilayer reflectivity using semiempirical methods.
  • Development and application of modified Darwin-Prins models for reflectivity analysis.
  • Utilizing a specialized spectrograph for absolute reflectivity measurements.
  • Implementation of computer programs for spectral analysis.

Main Results:

  • Detailed reflectivity characterizations for mica, potassium acid phthalate, Langmuir-Blodgett, and sputtered multilayers.
  • Derived analytical models accurately predict multilayer reflectivity and diffraction suppression.
  • Demonstrated the dependence of reflectivity on model parameters and interface structure.
  • Developed software for transforming measured spectra to absolute spectra.

Conclusions:

  • Multilayer analyzers are effective tools for absolute Bragg spectrometry in the 50-1000 eV range.
  • The developed analytical models and measurement procedures enable accurate X-ray source characterization.
  • This work provides a foundation for advanced applications in X-ray diagnostics and analysis.