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Screening of metal borohydrides by mechanochemistry and diffraction

Dorthe B Ravnsbæk1, Lise H Sørensen, Yaroslav Filinchuk

  • 1Center for Materials Crystallography, Interdisciplinary Nanoscience Center and Department of Chemistry, University of Aarhus, 8000 Aarhus C, Denmark.

Angewandte Chemie (International Ed. in English)
|March 3, 2012
PubMed
Abstract

No abstract available in PubMed .

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In addition to the oxymercuration–demercuration method, which converts the alkenes to alcohols with Markovnikov orientation, a complementary hydroboration-oxidation method yields the anti-Markovnikov product. The hydroboration reaction, discovered in 1959 by H.C. Brown, involves the addition of a B–H bond of borane to an alkene giving an organoborane intermediate. The oxidation of this intermediate with basic hydrogen peroxide forms an alcohol.