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Updated: Nov 11, 2025

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Evaluation of the Curing of Adhesive Systems by Rheological and Thermal Testing
Published on: July 3, 2020
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Back to the multi-step adhesive system: A next-generation two-step system with hydrophobic bonding agent improves
Azusa Yamanaka1, Atsushi Mine1, Mariko Matsumoto2,3
1Department of Fixed Prosthodontics, Osaka University Graduate School of Dentistry.
Dental Materials Journal
|March 29, 2021
Summary
A new hydrophobic bonding material (BZF-29) demonstrated superior long-term bonding effectiveness compared to existing systems. This dental adhesive showed significantly higher microtensile bond strength and improved failure modes, indicating enhanced durability.
Area of Science:
- Dental Materials Science
- Adhesive Dentistry
- Biomaterials Engineering
Background:
- Dental bonding agents are crucial for restorative procedures.
- Hydrophobic properties in bonding materials may enhance durability.
- Evaluating novel hydrophobic bonding systems is essential for improving clinical outcomes.
Purpose of the Study:
- To assess the bonding effectiveness of a new two-step hydrophobic bonding material (BZF-29).
- To compare the microtensile bond strength (µTBS) and failure modes of BZF-29 against established one-step and two-step bonding systems.
- To determine the long-term stability of the hydrophobic bonding system.
Main Methods:
- Microtensile bond strength (µTBS) testing was performed on three groups: BZF-29, G-Premio Bond (one-step), and CLEARFIL SE Bond 2 (two-step).
- Samples were aged in water for 24 hours, 3 months, and 6 months (n=25 per group).
- Fracture surfaces were analyzed using scanning electron microscopy (SEM) to characterize failure patterns.
Main Results:
- The BZF-29 group exhibited significantly higher µTBS than the GPB and SE2 groups (p<0.001).
- Dominant failure modes for BZF-29 were cohesive (48-84%), while GPB showed interface failure (48-52%) and SE2 showed mixed failure (48-60%).
- The hydrophobic nature of BZF-29 correlated with improved long-term bonding performance.
Conclusions:
- The novel two-step hydrophobic bonding material, BZF-29, offers superior long-term bonding effectiveness.
- Its hydrophobic characteristic contributes to enhanced durability and reduced interface failure.
- BZF-29 presents a promising advancement in dental adhesive technology for improved restorative longevity.

