Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

First principles simulations of transition metals for diodes: challenges and approaches to overcome inaccuracies in calculations.

Nanoscale advances·2026
Same author

Ultrafast carrier dynamics and electronic properties of PtSe<sub>2</sub>/MoSe<sub>2</sub> and WSe<sub>2</sub> 2D TMDC layered structures on mica: combined THz spectroscopy and DFT study.

RSC advances·2026
Same author

Tunable functional coverage of biocompatible magnesium silicate nanotubes by microwave-assisted silanization.

Nanoscale·2025
Same author

A novel experimental platform to monitor solid/water interfaces under freeze-thaw cycles.

Journal of microscopy·2025
Same author

Macroscopic and microscopic electron transfer kinetics of HOPG and graphite intercalated compound investigated by cyclic voltammetry and SECM.

Journal of microscopy·2025
Same author

Operando Exploration of CoAl-LDH: Transformations Driving Alkaline Oxygen Evolution Reaction.

Small (Weinheim an der Bergstrasse, Germany)·2025

Related Experiment Video

Updated: Sep 24, 2025

Fabrication of Gate-tunable Graphene Devices for Scanning Tunneling Microscopy Studies with Coulomb Impurities
11:42

Fabrication of Gate-tunable Graphene Devices for Scanning Tunneling Microscopy Studies with Coulomb Impurities

Published on: July 24, 2015

15.6K

Blisters on graphite surface: a scanning microwave microscopy investigation.

Eleonora Pavoni1, Rossella Yivlialin2, Christopher Hardly Joseph1

  • 1Department of Information Engineering, Università Politecnica delle Marche Ancona Italy e.pavoni@staff.univpm.it.

RSC Advances
|May 6, 2022
PubMed
Summary

Scanning microwave microscopy (SMM) offers sub-surface characterization of materials. This technique effectively studies electrochemical treatment-induced blisters on highly oriented pyrolytic graphite (HOPG) surfaces.

More Related Videos

Optimized Fabrication Procedure for High-Quality Graphene-based Moir&#233; Superlattice Devices
11:24

Optimized Fabrication Procedure for High-Quality Graphene-based Moiré Superlattice Devices

Published on: July 11, 2025

6.8K
Simultaneous Synthesis of Single-walled Carbon Nanotubes and Graphene in a Magnetically-enhanced Arc Plasma
09:48

Simultaneous Synthesis of Single-walled Carbon Nanotubes and Graphene in a Magnetically-enhanced Arc Plasma

Published on: February 2, 2012

15.4K

Related Experiment Videos

Last Updated: Sep 24, 2025

Fabrication of Gate-tunable Graphene Devices for Scanning Tunneling Microscopy Studies with Coulomb Impurities
11:42

Fabrication of Gate-tunable Graphene Devices for Scanning Tunneling Microscopy Studies with Coulomb Impurities

Published on: July 24, 2015

15.6K
Optimized Fabrication Procedure for High-Quality Graphene-based Moir&#233; Superlattice Devices
11:24

Optimized Fabrication Procedure for High-Quality Graphene-based Moiré Superlattice Devices

Published on: July 11, 2025

6.8K
Simultaneous Synthesis of Single-walled Carbon Nanotubes and Graphene in a Magnetically-enhanced Arc Plasma
09:48

Simultaneous Synthesis of Single-walled Carbon Nanotubes and Graphene in a Magnetically-enhanced Arc Plasma

Published on: February 2, 2012

15.4K

Area of Science:

  • Materials Science
  • Surface Science
  • Nanotechnology

Background:

  • Scanning microwave microscopy (SMM) probes material properties using microwave frequency electromagnetic fields.
  • SMM is often integrated with scanning probe microscopy (SPM) techniques for precise sample interaction.
  • The interaction involves an electromagnetic evanescent field and the sample surface.

Purpose of the Study:

  • To investigate blisters formed on highly oriented pyrolytic graphite (HOPG) surfaces after electrochemical treatment.
  • To demonstrate the capability of a home-made SMM setup for studying such surface phenomena.
  • To explore the sub-surface characterization potential of SMM.

Main Methods:

  • Coupling SMM with scanning tunneling microscopy (STM) to control probe-sample distance.
  • Utilizing the STM tip as an antenna for the microwave field.
  • Employing a broad-band SMM approach for local microwave spectroscopy across a wide frequency range.

Main Results:

  • The developed SMM system successfully characterized blisters on HOPG surfaces.
  • The broad-band approach enabled spectroscopy over a wide frequency range.
  • Microwave penetration allowed for the retrieval of sub-layer structural information.

Conclusions:

  • SMM is a suitable method for studying electrochemical treatment-induced surface features like blisters on HOPG.
  • The home-made broad-band SMM system provides valuable sub-surface insights.
  • Microwave penetration capabilities enhance material characterization beyond surface analysis.