Protocol for the synthesis of perovskite nanocrystal thin films via in situ crystallization method

The field of halide perovskites currently faces the challenge of finding an efficient approach for producing highly efficient and stable perovskite nanocrystals (PNCs). Here, we present a protocol for the annealing-free and antisolvent-free synthesis of PNCs. We describe the steps for preparing the PNCs precursor solutions. We then detail the procedures to control crucial processing parameters, such as the role of precursor concentration and the creation of humidity-controlled chambers, which allow achieving precise control over the final nanocrystals size. For complete details on the use and execution of this protocol, please refer to Noguera-Gómez et al.¹.