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Updated: Sep 18, 2025

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Evaluation of the Curing of Adhesive Systems by Rheological and Thermal Testing
Published on: July 3, 2020
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Could Tack-Curing Influence Margin Continuity and Conversion Degree of a Universal Dual-Curing Cement?
Leila Es Sebar1, Andrea Baldi2, Allegra Comba2
1Department of Applied Science and Technology, Politecnico di Torino, 10129 Turin, Italy.
Materials (Basel, Switzerland)
|June 27, 2025
Summary
Choosing the right polymerization protocol is key for dental crowns. A standard protocol improved marginal adaptation and conversion compared to tack curing, ensuring better restoration longevity.
Area of Science:
- Dental Materials Science
- Biomaterials Engineering
- Restorative Dentistry
Background:
- The long-term success of full-ceramic crowns relies heavily on proper polymerization of dental cements.
- Understanding the impact of different polymerization techniques on cement properties is essential for clinical application.
Purpose of the Study:
- To evaluate the effect of two distinct polymerization protocols on the marginal adaptation and degree of conversion (DC) of a universal dual-curing cement.
- To assess the influence of thermal aging on these properties.
Main Methods:
- Full-ceramic crowns (reinforced lithium silicate) were fabricated and cemented using a universal dual-curing cement.
- Two polymerization protocols were tested: G1 (microbrush excess removal, 1 min waiting, 20s light cure) and G2 (5s tack cure, scaler excess removal, 20s light cure).
- Marginal adaptation was analyzed using micro-computed tomography, and DC was measured via Raman spectroscopy before and after 10,000 thermal cycles.
Main Results:
- The tack-curing protocol (G2) resulted in significantly poorer marginal adaptation compared to the standard protocol (G1).
- No significant differences in marginal adaptation were observed between groups after thermal aging.
- Baseline DC was high across all samples, with no initial protocol-dependent variations. Thermal aging increased DC in the G1 group.
Conclusions:
- The selection of an appropriate polymerization protocol is critical for achieving optimal marginal adaptation in full-ceramic restorations.
- While both protocols yielded high initial DC, the standard protocol demonstrated superior marginal integrity, which was maintained after aging.
- Clinical recommendations should favor protocols ensuring better marginal seal to enhance restoration durability.
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